{"id":13958,"date":"2014-04-12T11:35:53","date_gmt":"2014-04-12T03:35:53","guid":{"rendered":"https:\/\/blog.kohan.com.tw\/?p=13958"},"modified":"2021-03-31T13:43:00","modified_gmt":"2021-03-31T05:43:00","slug":"%e5%85%a8%e8%87%aa%e5%8b%95%e9%a3%9f%e5%93%81%e4%b8%ad%e8%84%82%e8%82%aa%e7%b5%84%e6%88%90%e6%b8%ac%e5%ae%9a%ef%bc%9a%e7%b8%bd%e8%84%82%e8%82%aa%e3%80%81%e9%a3%bd%e5%92%8c%e8%84%82%e8%82%aa%e9%85%b8","status":"publish","type":"post","link":"https:\/\/blog.kohan.com.tw\/%e6%9c%89%e6%a9%9f%e5%88%86%e6%9e%90\/%e5%85%a8%e8%87%aa%e5%8b%95%e9%a3%9f%e5%93%81%e4%b8%ad%e8%84%82%e8%82%aa%e7%b5%84%e6%88%90%e6%b8%ac%e5%ae%9a%ef%bc%9a%e7%b8%bd%e8%84%82%e8%82%aa%e3%80%81%e9%a3%bd%e5%92%8c%e8%84%82%e8%82%aa%e9%85%b8\/","title":{"rendered":"\u5168\u81ea\u52d5\u98df\u54c1\u4e2d\u8102\u80aa\u7d44\u6210\u6e2c\u5b9a\uff1a\u7e3d\u8102\u80aa\u3001\u98fd\u548c\u8102\u80aa\u9178\u3001\u55ae\u5143\u4e0d\u98fd\u548c\u8102\u80aa\u9178\u3001\u53cd\u5f0f\u8102\u80aa\u9178"},"content":{"rendered":"

\u8102\u80aa\u9178\u5206\u6790\u524d\u8655\u7406\u5229\u5668\uff0d\u5168\u81ea\u52d5\u805a\u7126\u5f0f\u5fae\u6ce2\u6d88\u5316\u5668<\/h3>\n

\u8102\u80aa\u9178\u6aa2\u9a57\u7684\u91cd\u8981\u6027\u4e0d\u65b7\u589e\u52a0\uff0c\u9664\u98df\u54c1\u6a19\u7c64\u9700\u6e05\u695a\u6a19\u793a\u7e3d\u8102\u80aa\u3001\u98fd\u548c\u8102\u80aa\u9178\u3001\u55ae\u5143\u4e0d\u98fd\u548c\u8102\u80aa\u9178\u4ee5\u53ca\u53cd\u5f0f\u8102\u80aa\u9178\u7684\u7d44\u6210\u6bd4\u4f8b\u5916\uff0c.\u570b\u969b\u9593\u98df\u7528\u6cb9\u54c1\u4e4b\u9451\u5225\uff0c\u4ea6\u4ee5\u6aa2\u9a57\u8102\u80aa\u9178\u7d44\u6210\u70ba\u4e3b\u6d41\uff0c\u4e26\u85c9\u7531\u6bd4\u5c0d\u8cc7\u6599\u5eab\u9032\u884c\u7814\u5224\u3002\u8102\u80aa\u9178\u5178\u578b\u7684\u5206\u6790\u65b9\u5f0f\u5fc5\u9808\u5148\u4ee5\u7532\u9187\u8ff4\u6d41\u52a0\u71b1\u9032\u884c\u7682\u5316\u53cd\u61c9(\u4ee5Sodium Methoxide\u70ba\u50ac\u5316\u5291)\uff0c\u63a5\u8457\u4ee5\u4e09\u6c1f\u5316\u787c\u8ff4\u6d41\u916f\u5316\u6e38\u96e2\u8102\u80aa\u9178\uff0c\u6700\u5f8c\u5c07\u5df2\u8f49\u916f\u5316\u5b8c\u6210\u7684\u8102\u80aa\u9178\u7532\u916f(FAMEs)\u8403\u53d6\u51fa\u4f86\u4e26\u9664\u6c34\uff0c\u4fbf\u53ef\u4ee5\u6c23\u76f8\u5c64\u6790\u5100\u9032\u884c\u5206\u6790\u3002 \u55ae\u55ae\u7682\u5316\u8207\u8f49\u916f\u5316\u7684\u8ff4\u6d41\u6642\u9593\u4fbf\u9808\u82b1\u8cbb\u4e00\u500b\u5c0f\u6642\u5de6\u53f3\uff0c\u518d\u52a0\u4e0a\u5176\u4ed6\u5be6\u9a57\u7a0b\u5e8f\uff0c\u5f80\u5f80\u4e00\u500b\u5de5\u4f5c\u5929\u53ea\u80fd\u6e2c\u8a66\u4e00\u6279\u6a23\u54c1\u3002\u82e5\u85c9\u7531CEM Discover SP-D\u5168\u81ea\u52d5\u805a\u7126\u5f0f\u5fae\u6ce2\u6d88\u5316\u5668<\/a>\u53d6\u4ee3\u50b3\u7d71\u51b7\u51dd\u52a0\u71b1\u65b9\u5f0f\uff0c\u4fbf\u53ef\u5927\u5e45\u7e2e\u77ed\u52a0\u71b1\u6642\u9593\uff0c\u540c\u6642\u53ef\u907f\u514d\u4f7f\u7528\u4e0d\u6613\u6e05\u6d17\u4e7e\u6de8\u7684\u51b7\u51dd\u7ba1\uff0c\u518d\u914d\u5408GERSTEL MultiPurpose Sampler(MPS)\u591a\u529f\u80fd\u9032\u6a23\u7cfb\u7d71\uff0c\u4fbf\u80fd\u4ee5\u81ea\u52d5\u5316\u7684\u65b9\u5f0f\u5b8c\u6210\u7682\u5316\u3001\u8f49\u916f\u5316\u53ca\u8102\u80aa\u9178\u7532\u916f\u8403\u53d6\uff0c\u4e26\u81ea\u52d5\u5c07\u8403\u53d6\u7269\u5c0e\u5165GC-FID\u4e2d\u76f4\u63a5\u5206\u6790\uff0c1.5\u5c0f\u6642\u4fbf\u53ef\u5b8c\u6210\u50b3\u7d71\u65b9\u6cd5\u8981\u82b1\u4e00\u500b\u5de5\u4f5c\u5929\u624d\u80fd\u5b8c\u6210\u7684\u6a23\u54c1\u3002<\/p>\n<\/div>

\"fatty<\/span><\/div><\/div>
<\/div><\/div><\/div><\/div>

\u4ee5\u5168\u81ea\u52d5\u805a\u7126\u5f0f\u5fae\u6ce2\u6d88\u5316\u5668\u00a0\u9032\u884c\u8102\u80aa\u9178\u5206\u6790\u524d\u8655\u7406<\/h3>\n

\u5be6\u9a57\u8a2d\u5099\uff1a<\/h4>\n
    \n
  1. CEM Discover SP-D\u5fae\u6ce2\u6d88\u5316\u7cfb\u7d71<\/li>\n
  2. Agilent 7890\u6c23\u76f8\u5c64\u6790\u5100<\/li>\n
  3. Agilent\u706b\u7130\u96e2\u5b50\u5316\u5075\u6e2c\u5668(FID)<\/li>\n
  4. GERSTEL\u7a0b\u5f0f\u5347\u6eab\u6c7d\u5316\u9032\u6a23\u53e3(Proframmable Temperature Vaporization inlet, PTV inlet)<\/li>\n
  5. GERSTEL\u591a\u529f\u80fd\u9032\u6a23\u7cfb\u7d71(MultiPurpose Sampler, MPS)<\/li>\n<\/ol>\n<\/div>
    <\/span><\/div><\/div>
    \u57161. CEM Discover SP-D\u5fae\u6ce2\u6d88\u5316\u7cfb\u7d71\uff08\u5de6\uff09\uff1bDiscover SP-D\u7d50\u5408Agilent 7890 GC-FID\u8207GERSTEL PTV\/MPS\u591a\u529f\u80fd\u81ea\u52d5\u9032\u6a23\u7cfb\u7d71<\/h6><\/h6><\/div>
    <\/div><\/div><\/div><\/div>

    \u5be6\u9a57\u689d\u4ef6<\/h4>\n

    \u7a0b\u5f0f\u5347\u6eab\u6c7d\u5316\u9032\u6a23\u53e3\uff1abaffled liner\u3002split(50mL\/min)\u300240\u00b0C; 12\u00b0C\/s; 260\u00b0C(3 min)\u3002 \u7ba1\u67f1\uff1aAgilent 100 m CP Sil-88\u3002di=0.25 mm df=0.20 \u03bcm\u3002 \u8f09\u6d41\u6c23\u9ad4(He)\u6d41\u901f\uff1a1.2 mL\/min\u3002 \u8d77\u59cb\u6eab\u5ea6\uff1a80\u2103\uff0c\u6301\u7e8c2\u5206\u9418\u3002 \u5347\u6eab\u901f\u5ea6\uff1a80\u2103 \u4ee5\u6bcf\u5206\u94184\u2103\u5347\u6eab\u81f3225\u2103\u3002 \u6700\u7d42\u6eab\u5ea6\uff1a225\u2103\uff0c\u6301\u7e8c25\u5206\u9418\u3002 \u706b\u7130\u96e2\u5b50\u5316\u5075\u6e2c\u5668\u6eab\u5ea6\uff1a260\u00b0C\u3002 \u6a19\u6e96\u54c1\uff1aSupelco 37 component FAME standard (Catalog Number 47885-U)\u3002 \u6a23\u54c1\uff1a\u82b1\u751f\u3001\u7126\u7cd6\u3001\u5207\u9054\u8d77\u53f8\u3001\u8d77\u53f8\u7247\u3001\u512a\u683c\u3001\u852c\u83dc\u8d77\u53f8\u5976\u6cb9\u3001\u5de7\u514b\u529b\u3002\u53d60.1~0.3g\uff0c\u8207\u652a\u62cc\u5b50\u4e00\u8d77\u653e\u516535ml Pyrex\u5fae\u6ce2\u6d88\u5316\u74f6\u5167\uff0c\u84cb\u4e0a\u74f6\u84cb\u3002<\/p>\n

    \u81ea\u52d5\u5316\u6a23\u54c1\u8655\u7406\u7a0b\u5e8f<\/h4>\n

    1.\u52a0\u51651.0mL\u5167\u6a19\u6e96\u54c1\u6eb6\u6db2(Tritridecanoin in chloroform)\u3002 2.\u52a0\u51654mL\u76840.5N methanolic base\u3002 3.\u4ee580\u2103\u5fae\u6ce2\u52a0\u71b15\u5206\u9418\u3002 4.\u52a0\u51655mL BF3 in Methanol\u3002 5.\u4ee580\u2103\u5fae\u6ce2\u52a0\u71b15\u5206\u9418\u3002 6.\u52a0\u51655mL Hexane\u820710mL\u53bb\u96e2\u5b50\u6c34\u5f8c\uff0c\u652a\u62cc3\u5206\u9418\u3002 7.\u65bc\u4e002mL vial\u4e2d\u653e\u51650.2g\u786b\u9178\u9209\u3002 8.\u53d6\u51fa1mL Hexane\u5c64\u7684\u6a23\u54c1\u5230\u4e0a\u8ff02mL vial\u4e2d\u3002 9.\u4ee5500rpm\u652a\u62cc1\u5206\u9418\u3002 10.\u53d61.0 \u03bcL\u6ce8\u5165GC-FID\u4e2d\u3002<\/p>\n

    \u5168\u81ea\u52d5\u805a\u7126\u5f0f\u5fae\u6ce2\u6d88\u5316\u5668\u8207\u50b3\u7d71\u65b9\u6cd5\u4e4b\u6bd4\u8f03<\/h3>\n

    \u82b1\u751f\u3001\u7126\u7cd6\u8207\u5de7\u514b\u529b\u9032\u884c\u4e09\u91cd\u8907\u5be6\u9a57\uff0c\u5176\u4ed6\u6a23\u54c1\u5247\u9032\u884c\u96d9\u91cd\u8907\u5be6\u9a57\uff0c\u6e2c\u8a66\u7d50\u679c\u7d93\u6574\u7406\u8a08\u7b97\u5f8c\uff0c\u8207\u50b3\u7d71\u65b9\u6cd5\u7684\u6e2c\u8a66\u7d50\u679c\u5747\u653e\u5728\u4e0b\u88681\u3002\u7531\u8868\u4e2d\u7d50\u679c\u53ef\u5f97\u77e5\u4e0b\u5217\u7d50\u8ad6\uff1a<\/p>\n

      \n
    1. \u5de7\u514b\u529b\u3001\u82b1\u751f\u53ca\u7126\u7cd6\u5747\u9032\u884c\u4e09\u91cd\u8907\u6e2c\u8a66\uff0c\u76f8\u5c0d\u6a19\u6e96\u504f\u5dee(%RSD)\u5927\u591a\u4ecb\u65bc2~4%\uff0c\u986f\u793a\u5fae\u6ce2\u65b9\u6cd5\u5177\u826f\u597d\u91cd\u8907\u6027\u3002<\/li>\n
    2. \u8207\u50b3\u7d71\u65b9\u6cd5\u8207\u5fae\u6ce2\u65b9\u6cd5\u4e4b\u5206\u6790\u7d50\u679c\u5341\u5206\u76f8\u8fd1<\/li>\n<\/ol>\n<\/div>
      <\/span><\/div><\/div>
      \u88681. \u5168\u81ea\u52d5\u805a\u7126\u5f0f\u5fae\u6ce2\u6d88\u5316\u5668\u8207\u50b3\u7d71\u65b9\u6cd5\u4e4b\u8102\u80aa\u9178\u5206\u6790\u524d\u8655\u7406\u7d50\u679c\u6bd4\u8f03<\/h6><\/h6><\/div>
      <\/div><\/div><\/div><\/div>

      \u5168\u81ea\u52d5\u805a\u7126\u5f0f\u5fae\u6ce2\u6d88\u5316\u5668\u00a0\u5927\u5e45\u63d0\u5347\u8102\u80aa\u9178\u5206\u6790\u6548\u7387<\/h3>\n

      \u6bd4\u8f03\u50b3\u7d71\u65b9\u6cd5\u8207\u5168\u81ea\u52d5\u5fae\u6ce2\u6a23\u54c1\u524d\u8655\u7406\u65b9\u6cd5\u5f8c\uff0c\u5229\u7528\u5168\u81ea\u52d5\u5fae\u6ce2\u5206\u6790\u6a23\u54c1\u4e2d\u8102\u80aa\u9178\u7684\u6548\u7387\u70ba\u50b3\u7d71\u65b9\u6cd5\u7684\u4e94\u500d\u4ee5\u4e0a\uff0c\u53ea\u97001.5\u5c0f\u6642\u5373\u53ef\u5b8c\u6210\u50b3\u7d71\u65b9\u6cd5\u9700\u82b1\u8cbb\u4e00\u500b\u5de5\u4f5c\u5929\u624d\u80fd\u80fd\u5b8c\u6210\u7684\u6a23\u54c1\u91cf\uff0c\u5206\u6790\u7d50\u679c\u4ea6\u8207\u50b3\u7d71\u65b9\u6cd5\u76f8\u8fd1\uff0c\u63d0\u4f9b\u4e86\u50b3\u7d71\u8102\u80aa\u9178\u5206\u6790\u65b9\u5f0f\u5916\u7684\u53e6\u4e00\u7a2e\u66f4\u512a\u8cea\u7684\u5206\u6790\u9078\u64c7\u3002 <\/p>\n<\/div>

      <\/div><\/div><\/div><\/div><\/div>

      \u6b32\u4e86\u89e3\u66f4\u591a\u7684\u5100\u5668\u8cc7\u8a0a\u8207\u5be6\u9a57\u7d30\u7bc0\uff0c\u6b61\u8fce\u4f86\u96fb\u6d3d\u8a62 02-2728-2767\u6216 \u4f86\u4fe1<\/span><\/a><\/span>\u8207\u6211\u5011\u806f\u7e6b<\/p>\n<\/div>

      <\/div><\/div><\/div>

      \u6b32\u4e86\u89e3\u66f4\u591a\u7684\u5100\u5668\u8cc7\u8a0a\u8207\u5be6\u9a57\u7d30\u7bc0\uff0c\u6b61\u8fce\u4f86\u96fb\u6d3d\u8a62 02-2728-2767<\/a><\/span>\u6216 \u4f86\u4fe1<\/span><\/a><\/span>\u8207\u6211\u5011\u806f\u7e6b<\/p>\n<\/div>

      <\/div><\/div><\/div>

      \u53c3\u8003\u6587\u737b<\/h3><\/div>
        \n
      • Automated Determination of Total Fat, Saturated Fat, Monounsaturated Fat and Trans Fat Content in Food Samples. John R. Stuff, Jackie A. Whitecavage GERSTEL, Inc., 701 Digital Dr. Suite J, Linthicum, MD 21090, USA<\/li>\n<\/ul>\n<\/div>
        <\/div><\/div><\/div>
        <\/div><\/div><\/div><\/div><\/div><\/p>\n","protected":false},"excerpt":{"rendered":"","protected":false},"author":1,"featured_media":14225,"comment_status":"closed","ping_status":"closed","sticky":false,"template":"","format":"standard","meta":{"content-type":"","_monsterinsights_skip_tracking":false,"_monsterinsights_sitenote_active":false,"_monsterinsights_sitenote_note":"","_monsterinsights_sitenote_category":0,"footnotes":""},"categories":[71],"tags":[138,159,160],"acf":[],"yoast_head":"\n\u5168\u81ea\u52d5\u98df\u54c1\u4e2d\u8102\u80aa\u7d44\u6210\u6e2c\u5b9a\uff1a\u7e3d\u8102\u80aa\u3001\u98fd\u548c\u8102\u80aa\u9178\u3001\u55ae\u5143\u4e0d\u98fd\u548c\u8102\u80aa\u9178\u3001\u53cd\u5f0f\u8102\u80aa\u9178 | \u79d1\u5b89\u77e5\u8b58\u5eab<\/title>\n<meta name=\"robots\" content=\"index, follow, max-snippet:-1, max-image-preview:large, max-video-preview:-1\" \/>\n<link rel=\"canonical\" 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